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CHESS East
F2 Station

MacCHESS Scientist with F2 map

F2 Facility Description

The F2 station in CHESS East receives half of the powerful output from the positrons as they pass through the East 24-pole wiggler.  Since 1998 this station has been used primarily by the macromolecular crystallography users for multi-wavelength anomalous diffraction (MAD) measurements.  A new water cooled collimating mirror has been installed upstream of the monochromator to reduce the heat load and to provide better energy resolution for the user.  This station has a new double crystal monochromator as of 1999 to ease the transition to different energies.   The monochromator typically has a pair of vertically diffracting Si(111) crystals with the second crystal providing sagittal focusing in the horizontal dimension to focus ~2milliradians of beam to ~3.5mm.  The monochromator is designed to provide x-rays from 7.9 keV to 14 keV (0.89 - 1.57 Å).   The offset of the monochromated beam is 2.5 cm. downward from the white beam position. The vertical and horizontal beam sizes can be controlled by a pair of water cooled slit systems positioned in front of the monochromator, about 20.6 m from the wiggler.

For vertical focusing, a Rhodium coated silicon mirror is available (with a critical angle constant of 67 keV-mrad). It is located 3.3 meters upstream from the beryllium entrance window in the F2 hutch, which is 25.4 meters from the source, and can deflect the monochromated beam upward from 0 to 25 mrad without being obscured by the beryllium window holder.   Si(220) crystals are being constructed to provide even better energy resolution to the MAD user.

The F2 hutch houses a standard CHESS optical table with MacCHESS hardware and an ADSC Quantum-210 detector. The center of the hutch is 27.2 meters from the wiggler source and 6.5 meters from the F2 monochromator in the F-coffin.

F2 hutch

F2 station summary
 
Source: e+s, 24 pole wiggler, 1.7 mrad (horizontal)
Source size: FWHM (horizontal) = 3.76 mm, FWHM (vertical) = 0.944 mm
Distance to source: 27.2 m to center of hutch
Carbon filters: 0, 1, 2.5, 5, 10, 15, 25 mm (optional)
Cave slit sizes: 0 to 50 mm (horizontal), 0 to 12 mm (vertical)
Flux (100mA)(p/s): 8x1011 doubly-focused into 3.6 mm x 0.32 mm
 
Monochromators: Double-bounce downward, offset 25.4 mm
Crystals

Sag. Focus.

Energy
(keV)

/2 /3
Si (111) Yes 7.9-16 1.3

0.008

0.093

 
Monochromatic Mirrors:
Type Length Vertical Focus   E*c(keV-mrad)
Rh coated Si 24 inch Yes   67.0
Au-coated 9 inch No   80.0
Quartz 9 inch No   33.2
Float Glass 9 inch No   30.6
         
Typical Experiments:
Type
 
Energy Range

Equipment Setup
 

MAD

7.9-16 keV

Oscillation Camera, mirror #1

 

Last Update: 2006-09-21

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