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Chemical SOP - Acid Neutralization

Neutralization Procedures: 

General:  Do neutralizations in a fume hood behind a safety shield, as fumes and heat may be generated.

  • Wear lab coat or apron, gloves and goggles.

  • Keep containers cool during process.

  • Work slowly and carefully.

  • After neutralization is complete, flush to sewer with 20 parts water.

Acid Neutralization:  Use either a large Nalgene tub made of polyethylene or polycarbonate. Partially fill tub with cool water and sodium bi-carbonate.  Leave water running into the sink or into the Nalgene tub.

  1. While stirring, add acids slowly to tub.  When rapid reaction (bubbling) stops, stir to make sure all of the sodium bi-carbonate has reacted with the acid.

  2. If no sodium bi-carbonate is left in the tub, slowly add some more and stir until reaciotn stops.  Also add sodium bi-carbonate to the area around the container in the hood sink.

  3. When a pH of at least 5.5 is achieved, dispose of the solution into the sewer, followed by 20 parts water.  (Test with pH paper if necessary.)

  4. Be sure to wipe the area around the sink with a dampened sponge or lab wipe covered with sodium bi-carbonate to neutralize any spills.  After ensuring that all spills are neutralized, thoroughly rinse the hood sink and the hood counter to remove any sodium bicarbonate.

Prepared by:  David J. Jones
Date:  9 July, 2001

 

   

Last Update: 2006-09-21

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