Autonomous materials development using in situ laser annealing and scan-probe, grazing incident x-ray microdiffraction.
The experiment employed an AI-driven, fully autonomous infrastructure controlled across campus from CHESS to direct the synthesis and characterization in combinatorial thin-film material processing. Using high-throughput, closed-loop robotics, new materials were synthesized through laser-annealing, analyzed with x-ray diffraction, and the resulting data was fed into a machine-learning model to propose the next best experiment.